• Chinese Core Periodicals
  • Chinese Core Journals of Science and Technology
  • RCCSE Chinese Authoritative Academic Journals
ZHANG Liankun, WANG Yuefang, ZHANG Xiaoyu, et al. Effect on permeability of anthracite subjected to cyclical microwave modification[J]. Safety in Coal Mines, 2024, 55(6): 30−39. DOI: 10.13347/j.cnki.mkaq.20231225
Citation: ZHANG Liankun, WANG Yuefang, ZHANG Xiaoyu, et al. Effect on permeability of anthracite subjected to cyclical microwave modification[J]. Safety in Coal Mines, 2024, 55(6): 30−39. DOI: 10.13347/j.cnki.mkaq.20231225

Effect on permeability of anthracite subjected to cyclical microwave modification

More Information
  • Received Date: August 24, 2022
  • Revised Date: October 08, 2023
  • Increasing the permeability via microwaves is one of the potential feasible reservoir modification technologies to improve the efficiency of coalbed methane extraction. The microwave oven is used to conduct 3 cycles of microwave modification experiments on No.15 anthracite in Jincheng area of Qinshui Basin. The gas permeability of anthracite samples before and after each modification is tested using a self-built solid-gas coupling seepage platform. The pore properties are tested by micro CT scanning combined with image processing technology. In addition, the complexity index of pore-fracture network of coal samples before and after modification is discussed based on fractal theory. The results show that the gas permeability of anthracite sample increases with the increase of cycle times, and increases by 8.8 times after 3 cycles. The expansion and connection of pores/fractures in anthracite caused by microwave radiation is the fundamental reason for the increase of gas permeability. After three cycles, the total porosity of anthracite samples increases from 3.48% to 6.19%, in which the proportion of connected pores and fractures increases from 27.0% to 77.4%, and the proportion of isolated pores decreases from 73.0% to 22.6%. The pore number, pore volume, pore surface area and throat number, throat surface area and pore-throat coordination number of connected pores/fractures increase with the increase of cycle times, while the maximum throat length decreases, which confirms the “expansion and connection” effect of microwave modification on pores/fractures in anthracite. The two-dimensional fractal dimensions of pores/fractures of three typical sections in anthracite samples increase with the increase of cycle times, and increase from 1.25, 1.16, and 1.09 to 1.46, 1.54, and 1.37 respectively after three cycles, which clarifies that the cyclical microwave modification will make the pore-fracture network (gas seepage channel) in coal samples more complex.

  • [1]
    CAI Y D, LIU D M, PAN Z J. Partial coal pyrolysis and its implication to enhance coalbed methane recovery: A simulation study[J]. Energy & Fuels, 2017, 31(5): 4895−4903.
    [2]
    TENG T, WANG J G, GAO F, et al. Complex thermal coal-gas interactions in heat injection enhanced CBM recovery[J]. Journal of Natural Gas Science and Engineering, 2016, 34: 1174−1190. doi: 10.1016/j.jngse.2016.07.074
    [3]
    ZHAO Y S, MENG Q R, FENG Z C, et al. Evolving pore structures of lignite during pyrolysis observed by computed tomography[J]. Journal of Porous Media, 2017, 20(2): 143−153. doi: 10.1615/JPorMedia.v20.i2.40
    [4]
    LI H, SHI S L, LIN B Q, et al. A fully coupled electromagnetic, heat transfer and multiphase porous media model for microwave heating of coal[J]. Fuel Processing Technology, 2019, 189: 49−61. doi: 10.1016/j.fuproc.2019.03.002
    [5]
    LIN B Q, LI H, CHEN Z W, et al. Sensitivity analysis on the microwave heating of coal: A coupled electromagnetic and heat transfer model[J]. Applied Thermal Engineering, 2017, 126: 949−962. doi: 10.1016/j.applthermaleng.2017.08.012
    [6]
    李贺,林柏泉,洪溢都,等. 微波辐射下煤体孔裂隙结构演化特性[J]. 中国矿业大学学报,2017,46(6):1194−1201.

    LI He, LIN Baiquan, HONG Yidu, et al. Effect of microwave irradiation on pore and fracture evolutions of coal[J]. Journal of China University of Mining & Technolgy, 2017, 46(6): 1194−1201.
    [7]
    HONG Y D, LIN B Q, ZHU C J, et al. Effect of microwave irradiation on petrophysical characterization of coals[J]. Applied Thermal Engineering, 2016, 102: 1109−1125. doi: 10.1016/j.applthermaleng.2016.04.019
    [8]
    胡国忠,杨南,朱健,等. 微波辐射下含水分煤体孔渗特性及表面裂隙演化特征实验研究[J]. 煤炭学报,2020,45(S2):813−822.

    HU Guozhong, YANG Nan, ZHU Jian, et al. Evolution characteristics of microwave irradiation on pore-permeability and surface cracks of coal with water: An experimental study[J]. Journal of China Coal Society, 2020, 45(S2): 813−822.
    [9]
    HONG Y D, LIN B Q, LI H, et al. Three-dimensional simulation of microwave heating coal sample with varying parameters[J]. Applied Thermal Engineering, 2016, 93: 1145−1154. doi: 10.1016/j.applthermaleng.2015.10.041
    [10]
    XU G, HUANG J X, HU G Z, et al. Experimental study on effective microwave heating/fracturing of coal with various dielectric property and water saturation[J]. Fuel Processing Technology, 2020, 202: 106378. doi: 10.1016/j.fuproc.2020.106378
    [11]
    HUANG J X, XU G, CHEN Y P, et al. Simulation of microwave’s heating effect on coal seam permeability enhancement[J]. International Journal of Mining Science and Technology, 2019, 29(5): 785−789. doi: 10.1016/j.ijmst.2018.04.017
    [12]
    冯子军,赵阳升. 煤的热解破裂过程−孔裂隙演化的显微CT细观特征[J]. 煤炭学报,2015,40(1):103−108.

    FENG Zijun, ZHAO Yangsheng. Pyrolytic cracking in coal: Meso-characteristics of pore and fissure evolution observed by micro-CT[J]. Journal of China Coal Society, 2015, 40(1): 103−108.
    [13]
    康志勤,赵阳升,孟巧荣,等. 油页岩热破裂规律显微CT实验研究[J]. 地球物理学报,2009,52(3):842−848.

    KANG Zhiqin, ZHAO Yangsheng, MENG Qiaorong, et al. Micro-CT experimental research of oil shale thermal cracking laws[J]. Chinese Journal of Geophysics, 2009, 52(3): 842−848.
    [14]
    KONG X F, GUO J Q, KANG T H. Change of pore-fracture structure of anthracite modified by electrochemical treatment using micro-CT[J]. Advances in Materials Science and Engineering, 2018, 2018: 2651424.
    [15]
    YAO Y B, LIU D M, CHE Y, et al. Non-destructive characterization of coal samples from China using microfocus X-ray computed tomography[J]. International Journal of Coal Geology, 2009, 80(2): 113−123. doi: 10.1016/j.coal.2009.08.001
    [16]
    KUMAR H, LESTER E, KINGMAN S, et al. Inducing fractures and increasing cleat apertures in a bituminous coal under isotropic stress via application of microwave energy[J]. International Journal of Coal Geology, 2011, 88(1): 75−82. doi: 10.1016/j.coal.2011.07.007
    [17]
    ZHAO X C, BLUNT M J, YAO J. Pore-scale modeling: Effects of wettability on waterflood oil recovery[J]. Journal of Petroleum Science and Engineering, 2010, 71(3-4): 169−178. doi: 10.1016/j.petrol.2010.01.011
    [18]
    NGOM N F, GARNIER P, MONGA O, et al. Extraction of three-dimensional soil pore space from microtomography images using a geometrical approach[J]. Geoderma, 2011, 163(1-2): 127−134. doi: 10.1016/j.geoderma.2011.04.013
    [19]
    SILIN D, PATZEK T. Pore space morphology analysis using maximal inscribed spheres[J]. Physica A-Statistical Mechanics and Its Applications, 2006, 371(2): 336−360. doi: 10.1016/j.physa.2006.04.048
    [20]
    AL-KHARUSI A S, BLUNT M J. Network extraction from sandstone and carbonate pore space images[J]. Journal of Petroleum Science and Engineering, 2007, 56(4): 219−231. doi: 10.1016/j.petrol.2006.09.003
    [21]
    李一鸣,符世琛,焦亚博,等. 基于分形盒维数和小波包能量矩的垮落煤岩性状识别[J]. 煤炭学报,2017,42(3):803−808.

    LI Yiming, FU Shichen, JIAO Yabo, et al. Collapsing coal-rock identification based on fractal box dimension and wavelet packet energy moment[J]. Journal of China Coal Society, 2017, 42(3): 803−808.
    [22]
    傅雪海,李大华,秦勇,等. 煤基质收缩对渗透率影响的实验研究[J]. 中国矿业大学学报,2002,31(2):129−137. doi: 10.3321/j.issn:1000-1964.2002.02.005

    FU Xuehai, LI Dahua, QIN Yong, et al. Experimental research of influence of coal matrix shrinkage on permeability[J]. Journal of China University of Mining & Technology, 2002, 31(2): 129−137. doi: 10.3321/j.issn:1000-1964.2002.02.005
    [23]
    李俊乾,刘大锰,姚艳斌,等. 气体滑脱及有效应力对煤岩气相渗透率的控制作用[J]. 天然气地球科学,2013,24(5):1074−1078.

    LI Junqian, LIU Dameng, YAO Yanbin, et al. Controls of gas slippage and effective stress on the gas permeability of coal[J]. Natural Gas Geoscience, 2013, 24(5): 1074−1078.
    [24]
    LI J Q, LIU D M, YAO Y B, et al. Evaluation and modeling of gas permeability changes in anthracite coals[J]. Fuel, 2013, 111: 606−612. doi: 10.1016/j.fuel.2013.03.063
    [25]
    LI H Y, LAU H C, HUANG S. China’s coalbed methane development: A review of the challenges and opportunities in subsurface and surface engineering[J]. Journal of Petroleum Science and Engineering, 2018, 166: 621−635. doi: 10.1016/j.petrol.2018.03.047
    [26]
    LI Z, NI G H, WANG Y, et al. Semi-homogeneous model of coal based on 3D reconstruction of CT images and its seepage-deformation characteristics[J]. Energy, 2022, 259: 125044. doi: 10.1016/j.energy.2022.125044
    [27]
    翁斯灏. 烟煤中黄铁矿夹杂物的原位微波化学反应[J]. 华东师范大学学报(自然科学版),1996(3):46−51.

    WENG Sihao. Exploration on the mechanism of in-situ microwave chemical reaction of pyrite intrinsic in bituminous coal[J]. Journal of East China Normal University(Natural Science), 1996(3): 46−51.
    [28]
    QIN L, ZHAI C, LIU S M, et al. Fractal dimensions of low rank coal subjected to liquid nitrogen freeze-thaw based on nuclear magnetic resonance applied for coalbed methane recovery[J]. Powder Technology, 2018, 325: 11−20. doi: 10.1016/j.powtec.2017.11.027
  • Related Articles

    [1]REN Shaokui, QIN Yujin, JIA Zongkai, SU Weiwei, LI Zhenrong. Fractal characterization of pore structure of coal with different ranks and its effect on methane adsorption characteristics[J]. Safety in Coal Mines, 2023, 54(5): 175-181.
    [2]WANG Cuixia, REN Bang, LI Chengzhu. Heterogeneity characterization of coal pore structure with different metamorphic degrees[J]. Safety in Coal Mines, 2021, 52(6): 40-46.
    [3]LIU Jianhua, WANG Shengwei, SU Dongmei. Study on pore development characteristics of low rank coal reservoirs in Erlian Basin group[J]. Safety in Coal Mines, 2021, 52(2): 7-12.
    [4]LIU Yanwei, ZHANG Xinmiao, MIAO Jian. Study on Evolution of Pore Structure of Medium and High Rank Coals[J]. Safety in Coal Mines, 2020, 51(11): 7-13.
    [5]ZHANG Zhaozhao, PAN Jienan, LI Meng, WANG Kai. Total Pore Structure Characteristics of Coal with Different Metamorphic Degree Based on Joint Experiment of Mercury Intrusion and Low Temperature Nitrogen Adsorption[J]. Safety in Coal Mines, 2018, 49(4): 25-29.
    [6]XU Xin, XU Shuqi, XING Yueming, JIA Huimin. Study on Characterization Method of Fractal Features of Pore Structure for Coal Rock[J]. Safety in Coal Mines, 2018, 49(3): 148-150.
    [7]YU Liya. Reservoir Characteristic of Tectonic Coal and Its Influencing Factors in Changcun Coal Mine[J]. Safety in Coal Mines, 2018, 49(1): 176-178,182.
    [8]CHENG Liyuan, LI Wei. Tectonic Coal Matrix Compression Characteristics Based on Mercury Intrusion Method and Its Impact on Pore Structure[J]. Safety in Coal Mines, 2016, 47(2): 175-179.
    [9]WANG Hailong, LIU Hongfu, LI Wei, YANG Yali. Multifractal Characterization of Tectonically DeformedCoal Pore Structure Based on Mercury Injection Technology[J]. Safety in Coal Mines, 2016, 47(1): 33-37.
    [10]ZHANG Xiaohui, YAO Huifang, LI Wei. The Difference of Physical Properties of Tectonic Coal Reservoirs in Hancheng Block[J]. Safety in Coal Mines, 2014, 45(4): 176-179.
  • Cited by

    Periodical cited type(1)

    1. 李小刚,唐政,朱静怡,杨兆中,李扬,谢鹏,廖宇. 深层煤岩气压裂研究进展与展望. 天然气工业. 2024(10): 126-139 .

    Other cited types(1)

Catalog

    Article views (29) PDF downloads (7) Cited by(2)

    /

    DownLoad:  Full-Size Img  PowerPoint
    Return
    Return